Chemical Reaction Technologies Unit


The Chemical Reaction Technologies Unit provides ICIQ researchers with technical support in chemical reaction developement, with special emphasis on reaction parallelization and high throughput synthesis, reaction scale-out, in situ reaction monitoring, high pressure reactions and reactions performed in microflow reactors.


In the ambit of chemical parallelization, the Unit has equipment to cover all the unit operations involved in a chemical process: reaction, work-up, purification and final isolation of the product.
 
A chemical reaction can be scaled up, in a totally computer controlled reactor, from 0.6 to 6 L. This scale is optimal for preparing in-house starting materials and for technology transfer in cooperation projects.
 
In situ reaction monitoring can be performed either by heat flow calorimetry or by FTIR spectroscopy. These techniques are non intrusive and are very useful for kinetic and mechanistic studies.
 
Moreover the Unit provides ICIQ researchers with different technologies to perform reactions under singular conditions such as: a microwave reactor, photochemical reactor and a set of microflow reactions.

Equipment

Liquid phase parallel chemical synthesizer
Solid phase parallel chemical synthesizer
Platform for liquid additions
Platform for sequential liquid-liquid extraction and phase separation
Parallel centrifugal evaporator
Preparative flash chromatography system
Laboratory chemical reactor
FTIR monitoring system
Reaction calorimeter
Microwave reactor
Photochemical reactor
Ozone generator
Ball mill
Parallel pressure chemical synthesizer
High pressure reactors I
High pressure reactors II
Low pressure reactors I
Low pressure reactors II
Microreactors
  

Staff

 

DR. GISELA COLET I ESPAÑOL
UNIT MANAGER
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    Management and definition of the equipment and the unit.
Development of new applications in close collaboration with the researchers.
DR. MARTA GIMÉNEZ PEDRÓS
LABORATORY MANAGER
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    Development of new applications in close collaboration with the researchers.
Help the researchers using the Unit equipment and manteinance of the equipment.
MARIONA URTASUN PLANS
UNIT TECHNICIAN
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     Help the researchers using the Unit equipment and manteinance of the equipment.
DR. YVETTE A. MATA CAMPAÑA
UNIT TECHNICIAN
| contact |
     Help the researchers using the Unit equipment and manteinance of the equipment.

Seminars

9/8/2010 12:00
Prof. Alan Katritzky
University of Florida (USA)
Some recent developments in the synthesis of peptides and peptide conjugates
9/3/2010 12:00
Prof. Jaume Vilarrassa
Universitat de Barcelona
Catalytic tricks

Publications

Zinc acetates as efficient catalysts for the synthesis of bis-isocyanate precursors
E. Reixach, N. Bonet, F. X. Rius-Ruiz, S. Wershofen, A. Vidal-Ferran
Ind. Eng. Chem. Res. 2010, 49, 6362-6366
Through-space ligand interactions in enantiomeric dinuclear Ru complexes
N. Planas, G. J. Christian, E. Mas-Marzá, X. Sala, X. Fontrodona, F. Maseras, A. Llobet
Chem. Eur. J. 2010, 16, 7965-7968
Interplay between carbon monoxide, hydrides, and carbides in selective alkyne hydrogenation on palladium
M. García-Mota, B. Bridier, J. Pérez-Ramírez, N. López
J. Catal. 2010, 273, 92-102

News & Events

7/9/2010
2010 ICIQ Summer Fellows

Education

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