X-Ray Diffraction Unit


The X-ray Diffraction Unit gathers all the techniques together which are based on the diffraction of X-rays on crystalline solids.

The principal objective of the unit is giving support to the research groups and Crysforma Unit located at the ICIQ in the characterization of their chemical compounds which are available in a crystalline state.


Two principal techniques are available: Powder X-ray Diffraction (PXRD) and Single Crystal X-ray Diffraction (SCXRD).

The PXRD technique is used basically as a primary screening method and delivers a finger print of each different crystalline form analyzed. This method gives a basic service to all users at the ICIQ with a system which allows easy sample preparation and short measuring time for a high number of samples.

The SCXRD technique delivers a three-dimensional structure at atomic scale of a selected crystalline compound. This method is highly specialized with a system fitted together from high performance components. The objective in this case is to give a direct support to the research groups solving problems in all levels of difficulty. This support includes the crystallization of problematic samples, the preparation of crystals of poor quality and the refinement of troubling datasets.

Equipment

Powder X-ray diffraction system
Single crystal X-ray diffraction system
  

Staff

 

DR. JORDI BENET BUCHHOLZ
UNIT MANAGER
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    Management and definition of the unit and the equipment.
Development of new applications in close collaboration with the researchers.
EDUARDO ESCUDERO ADAN
UNIT TECHNICIAN
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    Operation and maintenance of the equipment.
Sample preparation, analysis and data interpretation.
Technical support to the researchers. 
MARTA MARTÍNEZ BELMONTE
UNIT TECHNICIAN
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Operation and maintenance of the equipment.
Sample preparation, analysis and data interpretation.
Technical support to the researchers. 

Seminars

3/26/2010 12:00
Prof. E. W. Meijer
Eindhoven University of Technology, The Netherlands
The non-covalent synthesis of functional supramolecular systems
3/19/2010 12:00
Prof. Jiri Srogl
Institute of Organic Chemistry and Biochemistry , Prague (Czech Republique)
Bio-inspired synthetic chemistry. From Cow Stomach to Apple
3/12/2010 12:00
Prof. Phil Gale
University of Southampton (UK)
New anion receptors and transporters

Publications

Bidimensional versus tridimensional oxygen vacancy diffusion in SnO2_x under different gas environments
N. López, J. D. Prades, F. Hernández-Ramírez, J. R. Morante, J. Pand, S. Mathur
Phys. Chem. Chem. Phys. 2010, 12, 2401-2406
Synthesis and photoisomerization of azocalixarenes with dendritic structures
H. Galán, G. Hennrich, J. de Mendoza, P. Prados
Eur. J. Org. Chem. 2010, 1249-1257
Perceptible influence of Pd and Pt heterocyclic carbene–pyridyl complexes in catalytic diboration of cyclic alkenes
C. Pubill-Ulldemolins, C. Bo, J. A. Mata, E. Fernández
Chem. Asian J. 2010, 5, 261-264

News & Events

3/4/2010
Call for 2010 ICIQ Summer Fellowships is now open
3/3/2010
Josep Albero, Master's Student Award
12/16/2009
ICIQ, awarded with the Narcís Monturiol Prize

Education

Go to EDUCATION